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›› 2018, Vol. 35 ›› Issue (6): 832-838.DOI: 10.7523/j.issn.2095-6134.2018.06.015

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Preparation of nano-TiO2 dispersion solution and its photocatalytic activity

WU Zhijiao1, ZHAI Yanqing2, GUO Rui2, CAO Baosheng2, PIAO Lingyu1   

  1. 1 Key Laboratory of Standardization and Measurement for Nanotechnology of Chinese Academy of Sciences, Center for Excellence in Nanoscience of Chinese Academy of Sciences, National Center for Nanoscience and Technology, Beijing 100190, China;
    2 School of Chemical Engineering, Beijing Institute of Petrochemical Technology, Beijing 102617, China
  • Received:2017-10-26 Revised:2017-12-07 Online:2018-11-15

Abstract: In this work, a kind of nano-TiO2 dispersion solution with excellent dispersity and stability was prepared and its photocatalytic activity was studied. The TiO2 nanoparticles (NPs) with particle size of 30nm were prepared using a combined method of precipitation and solvothermal. The morphology, structure, and surface state of TiO2 NPs were characterized by transmission electron microscope (TEM), scanning electron microscopy (SEM), X-ray powder diffraction (XRD), Fourier transform infrared spectra (FT-IR), and X-ray photoelectron spectroscopy (XPS). The results show that the TiO2 NPs are of anatase type with uniform particle size and good dispersion. Without surface modification, the prepared TiO2 dispersion solution keeps transparent after aged for 180 days at room temperature. Under UV irradiation, the dispersion shows excellent photocatalytic activity on degradation of rhodamine B. The aluminum substrates exhibit good self-cleaning ability after modification by the prepared dispersion.

Key words: TiO2 nanoparticles, dispersion, photocatalysis, dispersibility, stability

CLC Number: